European Conference of
CHEMICAL ENGINEERING (ECCE'11)

Puerto De La Cruz, Tenerife, December 10-12, 2011

 



 
 

 

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Photos from the same conferences of 2010

 

In Collaboration with the WSEAS
 

PROGRAM COMMITTEE:
(under confirmation)



H. Mandery, Belgium

L. M?dler, Denmark

P. A. Tanguy, France

M. V. Landau, Israel

J. ?t?p?nek, Czech Republic

M. Wichert, Denmark

J. P?idal,  Czech Republic

W. B. Krantz, USA

Jinghai Li, China

J. Ba?dyga, Poland

J. P. Meyer, South Africa

R. Costa, Portugal

D. G. Wood, Australia

Y. Matsumura, Japan

A. Cornell, Sweden

G. H. Kelsall, UK

K. Sundmacher, Denmark

M. Gehrig, Denmark

P. Mougin, France

J. I. Siepmann, USA

M. Ei?, Canada

J. W. Thybaut, Belgium

K. Jones, USA

C. Kennes, Spain

E. N. Lightfoot, USA











Plenary Lecture

Droplet-based Micro Continuous-Flow Synthesis and Combinatorial Optimization of Composed Nanoparticles

 


Professor Michael Kohler
Technical University Ilmenau
Institute of Micro- and Nanotechnologies
Institute for Physics
Ilmenau, Germany
E-mail: michael.koehler@tu-ilmenau.de


Abstract: A droplet-based synthesis concept offers several unique advantages for nanoparticle synthesis in comparison with the synthesis in homogeneous fluids, as constant residence times, suppression of undesired interactions between reactants, particles and the wall, support of efficient mixing and heat transfer by segment-internal convection. The possibility of precise control of changes of process conditions is of particular importance for multi step processes as nucleation, particle growth, particle aggregation and formation of shells. So, for example, different size, shape and optical properties of plasmonic Au/Ag particles can be addressed by tuning the conditions of microfluidic synthesis.
In addition, the micro segmented flow allows an efficient screening of large sets of reaction conditions by the definition of individual parameter sets in single nanoliter fluid segments. Two- three-, four- and five-dimensional concentration spaces are addressed by the application of computer-controlled syringe pumps for combinatorial experiments with several thousands single reaction volumes. The individual micro fluid segments with special reaction mixtures can be distinguished by their number in the segment sequence. The complete sets of synthesized colloidal solutions of nanoparticles were characterized by micro flow-through photometry and spectrophotometry. Selected products were further investigated by SEM, TEM, AFM and centrifugal sedimentation spectrometry. In result, homogeneous core/shell nanoparticles, double and triple shell nanoparticles as well as single crystal nanoparticles are synthesized under micro fluidic conditions.

Brief Biography of the Speaker:
J. Michael Kohler (born 1956) studied chemistry at the universities of Halle/S. and Jena. After dissertation on electrochemical effects in microfabrication (1986), he lead projects on submicron photolithography at the Institute of Physical Technology in Jena. During a research stay 1991 in Dortmund (MPG) he dealt with chemical waves in gels. He get the habilitation for general and physical chemistry of the university of Jena in 1992. In the same year, he become the head of the microfabrication department, in 1994 the head of the microsystem department of the Institute of Physical High Technology in Jena. Since 2001, he is a full professor for Physical Chemistry and Micro Reaction Technology at the Technical University of Ilmenau. His research activities are focussed on the connection between chip reactors, cell screening in microfluidic systems, biomolecular technologies, nanomaterials and nanotechnology.

 



NAUN: North Atlantic University Union